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Superconductivity, magnetism, and stoichiometry of single crystals of<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" display="inline"><mml:mrow><mml:msub><mml:mrow><mml:mtext>Fe</mml:mtext></mml:mrow><mml:mrow><mml:mn>1</mml:mn><mml:mo>+</mml:mo><mml:mi>y</mml:mi></mml:mrow></mml:msub><mml:msub><mml:mrow><mml:mrow><mml:mo>(</mml:mo><mml:mrow><mml:msub><mml:mrow><mml:mtext>Te</mml:mtext></mml:mrow><mml:mrow><mml:mn>1</mml:mn><mml:mo>−</mml:mo><mml:mi>x</mml:mi></mml:mrow></mml:msub><mml…
We report synthesis of high quality Fe1+y(Te1-xSx)z single crystals and a comprehensive study of structural, magnetic and transport properties. There is high sensitivity to material stoichiometry which includes vacancies on the Te(S) site. Our results reveal competition and coexistence of magnetic order and percolative superconductivity for x >= 0.03, while …